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Year 2024, Volume: 45 Issue: 3, 550 - 556, 30.09.2024

Nebiye Kızıl

https://doi.org/10.17776/csj.1525700

Abstract

References

  • [1] Cetinkaya A., Kaya,S. I., Ozcelikay-Akyildiz G., Ozkan S. A., Emerging analytical techniques in the analysis of food dyes, Green Chemistry in Food Analysis, Elsevier, (2024) 221-258.
  • [2] Sigurdson G. T., Tang P., Giusti M. M., Natural colorants: Food colorants from natural sources, Annu. Rev. Food Sci. Technol., 8(1) (2017) 261-280.
  • [3] Amchova P., Kotolova H., Ruda-Kucerova J., Health safety issues of synthetic food colorants. Regulatory toxicology and pharmacology, 73(3) (2015) 914-922.
  • [4] Erek F., Işik U., Meriç N., Synthesis and characterization of a novel ionic liquid for preconcentration of Brilliant Blue FCF (E 133) from some foods by ultrasound assisted temperature controlled ionic liquid dispersive liquid liquid microextraction method prior to spectrophotometric analysis; A comparative study, Food Chem., 445 (2024) 138694.
  • [5] Tutunaru B., Tigae C., Spînu C., Prunaru I., Spectrophotometry and electrochemistry of Brilliant Blue FCF in aqueous solution of NaX, Int. J. Electrochem. Sci., 12(1) (2017) 396-412.
  • [6] Gosetti F., Gianotti V., Angioi S., Polati S., Marengo E., Gennaro M. C., Oxidative degradation of food dye E133 Brilliant Blue FCF: liquid chromatography–electrospray mass spectrometry identification of the degradation pathway, J. Chromatogr. A, 1054(1-2) (2004) 379-387.
  • [7] Chakraborty A., Jayaseelan, K., Environmentally sustainable analytical quality by design aided RP-HPLC method for the estimation of brilliant blue in commercial food samples employing a green-ultrasound-assisted extraction technique, Green Process. Synth., 12(1) (2023) 20230178.
  • [8] Ferreira L. G. B., Faria R. X., Ferreira N. C. D. S., Soares-Bezerra R. J., Brilliant Blue Dyes in daily food: How could purinergic system be affected?, Int. J. Food Sci., 2016(1) (2016) 7548498.
  • [9] Lucarelli M. R., Shirk M. B., Julian M. W., Crouser E. D., Toxicity of Food Drug and Cosmetic Blue No. 1 dye in critically ill patients, Chest, 125(2) (2004) 793-795.
  • [10] [Guo J., Wu H., Du L., Fu Y., Determination of brilliant blue FCF in food and cosmetic samples by ionic liquid independent disperse liquid–liquid microextraction, Anal. Methods 5 (2013) 4021–4026.
  • [11] Pourali A., Abbasalizadeh A., Afshar Mogaddam M. R., Farajzadeh M. A., Tuzen M., Nemati M., Liquid Phase Microextraction of Hazardous Compounds in Dairy Products; Principal and Practical Aspects, Crit. Rev. Anal. Chem., (2023) 1-17.
  • [12] Kizil N., Basaran E., Erbilgin D., Yola M. L., Uzcan F., Soylak M., Deep eutectic solvent (DES) based dispersive Liquid-Phase microextraction of Sunset yellow FCF in food and pharmaceutical products, Microchem. J., 181 (2022) 107734.
  • [13] Yamini Y., Safari M., Shamsayei M., Simultaneous determination of steroid drugs in the ointment via magnetic solid phase extraction followed by HPLC-UV, J. Pharm. Anal., 8(4) (2018) 250-257.
  • [14] Samadi F., Sarafraz-Yazdi A., Es' haghi Z., An insight into the determination of trace levels of benzodiazepines in biometric systems: Use of crab shell powder as an environmentally friendly biosorbent, Journal of Chromatography B, 1092 (2018) 58-64.
  • [15] Islas G., Ibarra I. S., Hernandez P., Miranda J. M., Cepeda A., Dispersive solid phase extraction for the analysis of veterinary drugs applied to food samples: a review, J. Environ. Anal. Chem., 2017(1) (2017) 8215271.
  • [16] Qi L., Wang Y., Li Y., Zheng G., Li C., Su H., Microfluidic aqueous two-phase extraction of bisphenol A using ionic liquid for high-performance liquid chromatography analysis. Anal. Bioanal. Chem., 407 (2015) 3617-3625.
  • [17] Grau J., Azorín C., Benedé J. L., Chisvert A., Salvador A., Use of green alternative solvents in dispersive liquid‐liquid microextraction: A review, J. Sep. Sci., 45(1) (2022) 210-222.
  • [18] Rezaee M., Assadi Y., Hosseini M. R. M., Aghaee E., Ahmadi F., Berijani S., Determination of organic compounds in water using dispersive liquid–liquid microextraction, J. Chromatogr. A, 1116 (1-2) (2006) 1-9.
  • [19] Abbott A. P., Capper G., Davies D. L., Rasheed R. K., Tambyrajah, V., Novel solvent properties of choline chloride/urea mixtures, Chem. Commun., (1) (2003) 70-71.
  • [20] Vállez-Gomis V., Grau J., Benedé J. L., Giokas D. L., Chisvert A., Salvador A., Fundamentals and applications of stir bar sorptive dispersive microextraction: a tutorial review. Anal. Chim. Acta, 1153 (2021) 338271.
  • [21] Xu K., Wang Y., Huang Y., Li N., Wen Q., A green deep eutectic solvent-based aqueous two-phase system for protein extracting, Anal. Chim. Acta, 864 (2015) 9-20.
  • [22] Tang B., Zhang H., Row K. H., Application of deep eutectic solvents in the extraction and separation of target compounds from various samples, J. Sep. Sci., 38(6) (2015) 1053-1064.
  • [23] Chen J., Li Y., Wang X., Liu W., Application of deep eutectic solvents in food analysis: A review, Molecules, 24(24) (2019) 4594.
  • [24] Bişgin A. T., Selective separation and determination strategy for monitoring E100, E127, E129 and E133 in foodstuffs: Vortex assisted sequential-simultaneous liquid phase micro-extraction, Microchem. J., 196 (2024) 109716.
  • [25] Bogdanova P., Vakh C., Bulatov A., A surfactant-mediated microextraction of synthetic dyes from solid-phase food samples into the primary amine-based supramolecular solvent. Food Chem., 380 (2022) 131812.

Optimized Deep Eutectic Solvent System for Liquid Phase Microextraction of Brillant Blue FCF in Diverse Analytical Food Matrices

Year 2024, Volume: 45 Issue: 3, 550 - 556, 30.09.2024

Nebiye Kızıl

https://doi.org/10.17776/csj.1525700

Abstract

This study introduces a novel microextraction technique for the analysis of Brilliant Blue FCF, a widely used food dye, employing a deep eutectic solvent (DES). The method aligns with green chemistry principles by favoring environmentally benign solvents, ensuring rapid and efficient extraction. Specifically, a DES composed of tetrabutylammonium bromide (TBAB) and phenol (Ph) was prepared in a cost-effective and expedient manner. To enhance extraction efficiency within the deep eutectic solvent-based dispersive liquid-liquid microextraction (DB-DLLME), critical parameters such as the volume of DES, quantity of dispersive agent, extraction time, and sample volume were systematically optimized. The accuracy of the method was conducted at pH 3 by spiking various food samples with known concentrations of the analyte. Analytical performance metrics, including recovery efficiency, limit of detection (LOD), limit of quantification (LOQ), and relative standard deviation (RSD), were determined and reported as 0.86 µg/L, 2.88 µg/L, and 0.4-1.3% respectively. Furthermore, the method has been successfully utilized for analyzing samples of confectionery, beverages, water, and chewing gum.

Keywords

Deep eutectic solvent Spectrophotometric analysis Brillant blue FCF Green chemistry Food additives.

References

  • [1] Cetinkaya A., Kaya,S. I., Ozcelikay-Akyildiz G., Ozkan S. A., Emerging analytical techniques in the analysis of food dyes, Green Chemistry in Food Analysis, Elsevier, (2024) 221-258.
  • [2] Sigurdson G. T., Tang P., Giusti M. M., Natural colorants: Food colorants from natural sources, Annu. Rev. Food Sci. Technol., 8(1) (2017) 261-280.
  • [3] Amchova P., Kotolova H., Ruda-Kucerova J., Health safety issues of synthetic food colorants. Regulatory toxicology and pharmacology, 73(3) (2015) 914-922.
  • [4] Erek F., Işik U., Meriç N., Synthesis and characterization of a novel ionic liquid for preconcentration of Brilliant Blue FCF (E 133) from some foods by ultrasound assisted temperature controlled ionic liquid dispersive liquid liquid microextraction method prior to spectrophotometric analysis; A comparative study, Food Chem., 445 (2024) 138694.
  • [5] Tutunaru B., Tigae C., Spînu C., Prunaru I., Spectrophotometry and electrochemistry of Brilliant Blue FCF in aqueous solution of NaX, Int. J. Electrochem. Sci., 12(1) (2017) 396-412.
  • [6] Gosetti F., Gianotti V., Angioi S., Polati S., Marengo E., Gennaro M. C., Oxidative degradation of food dye E133 Brilliant Blue FCF: liquid chromatography–electrospray mass spectrometry identification of the degradation pathway, J. Chromatogr. A, 1054(1-2) (2004) 379-387.
  • [7] Chakraborty A., Jayaseelan, K., Environmentally sustainable analytical quality by design aided RP-HPLC method for the estimation of brilliant blue in commercial food samples employing a green-ultrasound-assisted extraction technique, Green Process. Synth., 12(1) (2023) 20230178.
  • [8] Ferreira L. G. B., Faria R. X., Ferreira N. C. D. S., Soares-Bezerra R. J., Brilliant Blue Dyes in daily food: How could purinergic system be affected?, Int. J. Food Sci., 2016(1) (2016) 7548498.
  • [9] Lucarelli M. R., Shirk M. B., Julian M. W., Crouser E. D., Toxicity of Food Drug and Cosmetic Blue No. 1 dye in critically ill patients, Chest, 125(2) (2004) 793-795.
  • [10] [Guo J., Wu H., Du L., Fu Y., Determination of brilliant blue FCF in food and cosmetic samples by ionic liquid independent disperse liquid–liquid microextraction, Anal. Methods 5 (2013) 4021–4026.
  • [11] Pourali A., Abbasalizadeh A., Afshar Mogaddam M. R., Farajzadeh M. A., Tuzen M., Nemati M., Liquid Phase Microextraction of Hazardous Compounds in Dairy Products; Principal and Practical Aspects, Crit. Rev. Anal. Chem., (2023) 1-17.
  • [12] Kizil N., Basaran E., Erbilgin D., Yola M. L., Uzcan F., Soylak M., Deep eutectic solvent (DES) based dispersive Liquid-Phase microextraction of Sunset yellow FCF in food and pharmaceutical products, Microchem. J., 181 (2022) 107734.
  • [13] Yamini Y., Safari M., Shamsayei M., Simultaneous determination of steroid drugs in the ointment via magnetic solid phase extraction followed by HPLC-UV, J. Pharm. Anal., 8(4) (2018) 250-257.
  • [14] Samadi F., Sarafraz-Yazdi A., Es' haghi Z., An insight into the determination of trace levels of benzodiazepines in biometric systems: Use of crab shell powder as an environmentally friendly biosorbent, Journal of Chromatography B, 1092 (2018) 58-64.
  • [15] Islas G., Ibarra I. S., Hernandez P., Miranda J. M., Cepeda A., Dispersive solid phase extraction for the analysis of veterinary drugs applied to food samples: a review, J. Environ. Anal. Chem., 2017(1) (2017) 8215271.
  • [16] Qi L., Wang Y., Li Y., Zheng G., Li C., Su H., Microfluidic aqueous two-phase extraction of bisphenol A using ionic liquid for high-performance liquid chromatography analysis. Anal. Bioanal. Chem., 407 (2015) 3617-3625.
  • [17] Grau J., Azorín C., Benedé J. L., Chisvert A., Salvador A., Use of green alternative solvents in dispersive liquid‐liquid microextraction: A review, J. Sep. Sci., 45(1) (2022) 210-222.
  • [18] Rezaee M., Assadi Y., Hosseini M. R. M., Aghaee E., Ahmadi F., Berijani S., Determination of organic compounds in water using dispersive liquid–liquid microextraction, J. Chromatogr. A, 1116 (1-2) (2006) 1-9.
  • [19] Abbott A. P., Capper G., Davies D. L., Rasheed R. K., Tambyrajah, V., Novel solvent properties of choline chloride/urea mixtures, Chem. Commun., (1) (2003) 70-71.
  • [20] Vállez-Gomis V., Grau J., Benedé J. L., Giokas D. L., Chisvert A., Salvador A., Fundamentals and applications of stir bar sorptive dispersive microextraction: a tutorial review. Anal. Chim. Acta, 1153 (2021) 338271.
  • [21] Xu K., Wang Y., Huang Y., Li N., Wen Q., A green deep eutectic solvent-based aqueous two-phase system for protein extracting, Anal. Chim. Acta, 864 (2015) 9-20.
  • [22] Tang B., Zhang H., Row K. H., Application of deep eutectic solvents in the extraction and separation of target compounds from various samples, J. Sep. Sci., 38(6) (2015) 1053-1064.
  • [23] Chen J., Li Y., Wang X., Liu W., Application of deep eutectic solvents in food analysis: A review, Molecules, 24(24) (2019) 4594.
  • [24] Bişgin A. T., Selective separation and determination strategy for monitoring E100, E127, E129 and E133 in foodstuffs: Vortex assisted sequential-simultaneous liquid phase micro-extraction, Microchem. J., 196 (2024) 109716.
  • [25] Bogdanova P., Vakh C., Bulatov A., A surfactant-mediated microextraction of synthetic dyes from solid-phase food samples into the primary amine-based supramolecular solvent. Food Chem., 380 (2022) 131812.
There are 25 citations in total.

Details

Primary Language English
Subjects Analytical Spectrometry, Instrumental Methods, Analytical Chemistry (Other)
Journal Section Natural Sciences
Authors

Nebiye Kızıl 0000-0003-4994-1680

Publication Date September 30, 2024
Submission Date July 31, 2024
Acceptance Date September 23, 2024
Published in Issue Year 2024Volume: 45 Issue: 3

Cite

APA Kızıl, N. (2024). Optimized Deep Eutectic Solvent System for Liquid Phase Microextraction of Brillant Blue FCF in Diverse Analytical Food Matrices. Cumhuriyet Science Journal, 45(3), 550-556. https://doi.org/10.17776/csj.1525700
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