Optimized Deep Eutectic Solvent System for Liquid Phase Microextraction of Brillant Blue FCF in Diverse Analytical Food Matrices

Nebiye Kızıl

doi:10.17776/csj.1525700

EN

Optimized Deep Eutectic Solvent System for Liquid Phase Microextraction of Brillant Blue FCF in Diverse Analytical Food Matrices

Abstract

This study introduces a novel microextraction technique for the analysis of Brilliant Blue FCF, a widely used food dye, employing a deep eutectic solvent (DES). The method aligns with green chemistry principles by favoring environmentally benign solvents, ensuring rapid and efficient extraction. Specifically, a DES composed of tetrabutylammonium bromide (TBAB) and phenol (Ph) was prepared in a cost-effective and expedient manner. To enhance extraction efficiency within the deep eutectic solvent-based dispersive liquid-liquid microextraction (DB-DLLME), critical parameters such as the volume of DES, quantity of dispersive agent, extraction time, and sample volume were systematically optimized. The accuracy of the method was conducted at pH 3 by spiking various food samples with known concentrations of the analyte. Analytical performance metrics, including recovery efficiency, limit of detection (LOD), limit of quantification (LOQ), and relative standard deviation (RSD), were determined and reported as 0.86 µg/L, 2.88 µg/L, and 0.4-1.3% respectively. Furthermore, the method has been successfully utilized for analyzing samples of confectionery, beverages, water, and chewing gum.

Keywords

References

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Details

Primary Language

English

Subjects

Analytical Spectrometry , Instrumental Methods , Analytical Chemistry (Other)

Journal Section

Research Article

Authors

Nebiye Kızıl ^*
0000-0003-4994-1680
Türkiye

Publication Date

September 30, 2024

Submission Date

July 31, 2024

Acceptance Date

September 23, 2024

Published in Issue

Year 2024 Volume: 45 Number: 3

DOI

https://doi.org/10.17776/csj.1525700

IZ

https://izlik.org/JA66DB56DJ

Cite

RIS / Bibtex

APA

Kızıl, N. (2024). Optimized Deep Eutectic Solvent System for Liquid Phase Microextraction of Brillant Blue FCF in Diverse Analytical Food Matrices. Cumhuriyet Science Journal, 45(3), 550-556. https://doi.org/10.17776/csj.1525700

Cited By

Natural Deep Eutectic Solvents in Extraction Science: Progress, Challenges, and Future Prospects

SEPARATION SCIENCE PLUS

https://doi.org/10.1002/sscp.70075

Öz

Optimized Deep Eutectic Solvent System for Liquid Phase Microextraction of Brillant Blue FCF in Diverse Analytical Food Matrices

Abstract

Keywords

References

Details

Primary Language

Subjects

Journal Section

Authors

Publication Date

Submission Date

Acceptance Date

Published in Issue

DOI

IZ

Cite

Cited By

Natural Deep Eutectic Solvents in Extraction Science: Progress, Challenges, and Future Prospects