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Sensitive Determination of Venlafaxine in Urine Samples by Using HPLC-DAD System After Fabric Phase Sorptive Extraction

Year 2022, Volume: 43 Issue: 4, 600 - 605, 27.12.2022

Beyzanur Özdemir , Halil İbrahim Ulusoy , Ümmügülsüm Morgül , Marcello Locatelli , Abuzar Kabir

https://doi.org/10.17776/csj.1182848
Cited By: 2

Abstract

This study is focused on developing a sensitive analytical method for Venlafaxine molecule which is antidepressant drug belonging to the serotonin-noradrenaline reuptake inhibitors (SNRI) group. With this study, a separation and preconcentration method based on fabric phase sorptive extraction(FPSE) method was developed for low levels of Venlafaxine in urine samples. Experimental variables such as pH, ionic strength, desorption solvent, and other parameters were studied and optimized step by step. The linearity of method under optimized conditions is in the range of 15.00-750.00 ng mL-1 while limit of detection is 4.28 ng mL-1. The relative standard deviation (RSD %) obtained from model solutions containing 300 ng mL-1 of Venlafaxine was lower than 3.1 % and pre-concentration factor was calculated as 62.50 for target molecule. In order to test accuracy of the method, recovery tests were carried out by means of spiked urine samples. As a result of recovery tests, quantative values were obtained in the range of 97.5-104.2 % successively.

Keywords

HPLC Fabric phase sorptive extraction Venlafaxine Analytical method development

Supporting Institution

Tubitak

References

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  • [2] A.R. Chaves, S.M. Silva, R.H.C. Queiroz, F.M. Lanças, M.E.C. Queiroz, Stir bar sorptive extraction and liquid chromatography with UV detection for determination of antidepressants in plasma samples, J. Chromatogr. B Anal. Technol. Biomed. Life Sci.,850 (2007) 295-302.
  • [3] N. Dilbaz, A.R. Özen, M. Ay, H. Güz, S. Karademir, Venlafaksin’in major depresyonda etkinlik ve emniyeti; ümitsizlik, intihar düşüncesi ve anksiyete üzerine etkisi: Bir açık çalışma, Psikofarmakoloji. Org., 9 (1999) 197–202.
  • [4] H. Juan, Z. Zhiling, L. Huande, Simultaneous determination of fluoxetine, citalopram, paroxetine, venlafaxine in plasma by high performance liquid chromatography-electrospray ionization mass spectrometry (HPLC-MS/ESI), J. Chromatogr. B Anal. Technol. Biomed. Life Sci.,820 (2005) 33-39.
  • [5] S. Rani, A.K. Malik, R. Kaur, R. Kaur, A Review for the Analysis of Antidepressant, Antiepileptic and Quinolone Type Drugs in Pharmaceuticals and Environmental Samples, Crit. Rev. Anal. Chem.,46 (2016) 424-442.
  • [6] A. Khan, Vilazodone, a novel dual-acting serotonergic antidepressant for managing major depression, Expert Opin. Investig. Drugs.,18 (2009) 1753-1764.
  • [7] P.L. Kole, G. Venkatesh, J. Kotecha, R. Sheshala, Recent advances in sample preparation techniques for effective bioanalytical methods, Biomed. Chromatogr., 25 (2011) 199-217.
  • [8] A.G. Canlı, B. Sürücü, H.I. Ulusoy, E. Yılmaz, A. Kabir, M. Locatelli, Analytical methodology for trace determination of propoxur and fenitrothion pesticide residues by decanoic acid modified magnetic nanoparticles, Molecule, 24 (2019) 4621.
  • [9] E. Karaca, S. Ulusoy, U. Morgül, H.İ. Ulusoy, Development of Analytical Method for Sensitive Determination of Streptozotocin based on Solid Phase Extraction, Cumhuriyet Sci. J., 41 (2020) 826–831.
  • [10] S. Ulusoy, M. Locatelli, A. Tartaglia, A. Kabir, H.İ. Ulusoy, Sensitive determination of Anastrozole and Letrozole in urine samples by novel magnetic nanoparticles containing tetraethylenepentamine ( TEPA ) prior to analysis by high performance liquid chromatography diode array detection, Chem. Pap., 76 (2022) 3649–3659.
  • [11] M. Sarıkaya, H.I. Ulusoy, U. Morgul, S. Ulusoy, A. Tartaglia, E. Yılmaz, M. Soylak, M. Locatelli, A. Kabir, Sensitive determination of Fluoxetine and Citalopram antidepressants in urine and wastewater samples by liquid chromatography coupled with photodiode array detector, J. Chromatogr. A., 1648 (2021) 462215.
  • [12] A. Kabir, R. Mesa, J. Jurmain, K. Furton, Fabric Phase Sorptive Extraction Explained, Separations., 4 (2017) 21.
  • [13] V. Kazantzi, A. Anthemidis, Fabric sol–gel phase sorptive extraction technique: A review, Separations, 4 (2017) 1–20.
  • [14] E. Agadellis, A. Tartaglia, M. Locatelli, A. Kabir, K.G. Furton, V. Samanidou, Mixed-mode fabric phase sorptive extraction of multiple tetracycline residues from milk samples prior to high performance liquid chromatography-ultraviolet analysis, Microchem. J., 159 (2020) 105437.
  • [15] E. Zilfidou, A. Kabir, K.G. Furton, V. Samanidou, An improved fabric phase sorptive extraction method for the determination of five selected antidepressant drug residues in human blood serum prior to high performance liquid chromatography with diode array detection, J. Chromatogr. B Anal. Technol. Biomed. Life Sci., 1125 (2019) 1–11.
  • [16] A. Kabir, R. Mesa, J. Jurmain, K. Furton, Fabric Phase Sorptive Extraction Explained, Separations, 4 (2017) 21.
  • [17] V. Samanidou, K. Michaelidou, A. Kabir, K.G. Furton, Fabric phase sorptive extraction of selected penicillin antibiotic residues from intact milk followed by high performance liquid chromatography with diode array detection, Food Chem., 224 (2017) 131-138.
  • [18] S. Gülle, H.I. Ulusoy, A. Kabir, A. Tartaglia, K.G. Furton, M. Locatelli, V.F. Samanidou, Application of a fabric phase sorptive extraction-high performance liquid chromatography-photodiode array detection method for the trace determination of methyl paraben, propyl paraben and butyl paraben in cosmetic and environmental samples, Anal. Methods., 11 (2019) 6136–6145.
  • [19] A. Tartaglia, M. Locatelli, A. Kabir, K.G. Furton, D. Macerola, E. Sperandio, S. Piccolantonio, H.I. Ulusoy, F. Maroni, P. Bruni, F. Croce, V.F. Samanidou, Comparison between exhaustive and equilibrium extraction using different SPE sorbents and sol-gel carbowax 20M coated FPSE media, Molecule, 24 (2019) 382.
  • [20] A. Kabir, K.G. Furton, N. Tinari, L. Grossi, D. Innosa, D. Macerola, A. Tartaglia, V. Di Donato, C. D’Ovidio, M. Locatelli, Fabric phase sorptive extraction-high performance liquid chromatography-photo diode array detection method for simultaneous monitoring of three inflammatory bowel disease treatment drugs in whole blood, plasma and urine, J. Chromatogr. B Anal. Technol. Biomed. Life Sci.,1084 (2018) 53-63.
  • [21] H.I. Ulusoy, S. Gülle, E. Yilmaz, M. Soylak, Trace determination of vitamin B12 in food samples by using Fe3O4 magnetic particles including multi-walled carbon nanotubes and nanodiamonds, Anal. Methods, 11 (2019) 5108–5117.
  • [22] N.F. de Rosa, N.A. Sharley, Stability of venlafaxine hydrochloride liquid formulations suitable for administration via enteral feeding tubes, J. Pharm. Pract. Res., 38 (2008) 212–215.

Year 2022, Volume: 43 Issue: 4, 600 - 605, 27.12.2022

Beyzanur Özdemir , Halil İbrahim Ulusoy , Ümmügülsüm Morgül , Marcello Locatelli , Abuzar Kabir

https://doi.org/10.17776/csj.1182848
Cited By: 2

Abstract

References

  • [1] M. Leblanc, L. Thibault, Effect of sibutramine on macronutrient selection in male and female rats, Physiol. Behav.,80 (2003) 243–252.
  • [2] A.R. Chaves, S.M. Silva, R.H.C. Queiroz, F.M. Lanças, M.E.C. Queiroz, Stir bar sorptive extraction and liquid chromatography with UV detection for determination of antidepressants in plasma samples, J. Chromatogr. B Anal. Technol. Biomed. Life Sci.,850 (2007) 295-302.
  • [3] N. Dilbaz, A.R. Özen, M. Ay, H. Güz, S. Karademir, Venlafaksin’in major depresyonda etkinlik ve emniyeti; ümitsizlik, intihar düşüncesi ve anksiyete üzerine etkisi: Bir açık çalışma, Psikofarmakoloji. Org., 9 (1999) 197–202.
  • [4] H. Juan, Z. Zhiling, L. Huande, Simultaneous determination of fluoxetine, citalopram, paroxetine, venlafaxine in plasma by high performance liquid chromatography-electrospray ionization mass spectrometry (HPLC-MS/ESI), J. Chromatogr. B Anal. Technol. Biomed. Life Sci.,820 (2005) 33-39.
  • [5] S. Rani, A.K. Malik, R. Kaur, R. Kaur, A Review for the Analysis of Antidepressant, Antiepileptic and Quinolone Type Drugs in Pharmaceuticals and Environmental Samples, Crit. Rev. Anal. Chem.,46 (2016) 424-442.
  • [6] A. Khan, Vilazodone, a novel dual-acting serotonergic antidepressant for managing major depression, Expert Opin. Investig. Drugs.,18 (2009) 1753-1764.
  • [7] P.L. Kole, G. Venkatesh, J. Kotecha, R. Sheshala, Recent advances in sample preparation techniques for effective bioanalytical methods, Biomed. Chromatogr., 25 (2011) 199-217.
  • [8] A.G. Canlı, B. Sürücü, H.I. Ulusoy, E. Yılmaz, A. Kabir, M. Locatelli, Analytical methodology for trace determination of propoxur and fenitrothion pesticide residues by decanoic acid modified magnetic nanoparticles, Molecule, 24 (2019) 4621.
  • [9] E. Karaca, S. Ulusoy, U. Morgül, H.İ. Ulusoy, Development of Analytical Method for Sensitive Determination of Streptozotocin based on Solid Phase Extraction, Cumhuriyet Sci. J., 41 (2020) 826–831.
  • [10] S. Ulusoy, M. Locatelli, A. Tartaglia, A. Kabir, H.İ. Ulusoy, Sensitive determination of Anastrozole and Letrozole in urine samples by novel magnetic nanoparticles containing tetraethylenepentamine ( TEPA ) prior to analysis by high performance liquid chromatography diode array detection, Chem. Pap., 76 (2022) 3649–3659.
  • [11] M. Sarıkaya, H.I. Ulusoy, U. Morgul, S. Ulusoy, A. Tartaglia, E. Yılmaz, M. Soylak, M. Locatelli, A. Kabir, Sensitive determination of Fluoxetine and Citalopram antidepressants in urine and wastewater samples by liquid chromatography coupled with photodiode array detector, J. Chromatogr. A., 1648 (2021) 462215.
  • [12] A. Kabir, R. Mesa, J. Jurmain, K. Furton, Fabric Phase Sorptive Extraction Explained, Separations., 4 (2017) 21.
  • [13] V. Kazantzi, A. Anthemidis, Fabric sol–gel phase sorptive extraction technique: A review, Separations, 4 (2017) 1–20.
  • [14] E. Agadellis, A. Tartaglia, M. Locatelli, A. Kabir, K.G. Furton, V. Samanidou, Mixed-mode fabric phase sorptive extraction of multiple tetracycline residues from milk samples prior to high performance liquid chromatography-ultraviolet analysis, Microchem. J., 159 (2020) 105437.
  • [15] E. Zilfidou, A. Kabir, K.G. Furton, V. Samanidou, An improved fabric phase sorptive extraction method for the determination of five selected antidepressant drug residues in human blood serum prior to high performance liquid chromatography with diode array detection, J. Chromatogr. B Anal. Technol. Biomed. Life Sci., 1125 (2019) 1–11.
  • [16] A. Kabir, R. Mesa, J. Jurmain, K. Furton, Fabric Phase Sorptive Extraction Explained, Separations, 4 (2017) 21.
  • [17] V. Samanidou, K. Michaelidou, A. Kabir, K.G. Furton, Fabric phase sorptive extraction of selected penicillin antibiotic residues from intact milk followed by high performance liquid chromatography with diode array detection, Food Chem., 224 (2017) 131-138.
  • [18] S. Gülle, H.I. Ulusoy, A. Kabir, A. Tartaglia, K.G. Furton, M. Locatelli, V.F. Samanidou, Application of a fabric phase sorptive extraction-high performance liquid chromatography-photodiode array detection method for the trace determination of methyl paraben, propyl paraben and butyl paraben in cosmetic and environmental samples, Anal. Methods., 11 (2019) 6136–6145.
  • [19] A. Tartaglia, M. Locatelli, A. Kabir, K.G. Furton, D. Macerola, E. Sperandio, S. Piccolantonio, H.I. Ulusoy, F. Maroni, P. Bruni, F. Croce, V.F. Samanidou, Comparison between exhaustive and equilibrium extraction using different SPE sorbents and sol-gel carbowax 20M coated FPSE media, Molecule, 24 (2019) 382.
  • [20] A. Kabir, K.G. Furton, N. Tinari, L. Grossi, D. Innosa, D. Macerola, A. Tartaglia, V. Di Donato, C. D’Ovidio, M. Locatelli, Fabric phase sorptive extraction-high performance liquid chromatography-photo diode array detection method for simultaneous monitoring of three inflammatory bowel disease treatment drugs in whole blood, plasma and urine, J. Chromatogr. B Anal. Technol. Biomed. Life Sci.,1084 (2018) 53-63.
  • [21] H.I. Ulusoy, S. Gülle, E. Yilmaz, M. Soylak, Trace determination of vitamin B12 in food samples by using Fe3O4 magnetic particles including multi-walled carbon nanotubes and nanodiamonds, Anal. Methods, 11 (2019) 5108–5117.
  • [22] N.F. de Rosa, N.A. Sharley, Stability of venlafaxine hydrochloride liquid formulations suitable for administration via enteral feeding tubes, J. Pharm. Pract. Res., 38 (2008) 212–215.
There are 22 citations in total.

Details

Primary Language English
Subjects Pharmacology and Pharmaceutical Sciences
Journal Section Natural Sciences
Authors

Beyzanur Özdemir 0000-0002-0634-837X

Halil İbrahim Ulusoy 0000-0002-8742-5145

Ümmügülsüm Morgül 0000-0001-8393-2396

Marcello Locatelli 0000-0002-0840-825X

Abuzar Kabir 0000-0002-3740-8857

Publication Date December 27, 2022
Submission Date October 1, 2022
Acceptance Date December 9, 2022
Published in Issue Year 2022Volume: 43 Issue: 4

Cite

APA Özdemir, B., Ulusoy, H. İ., Morgül, Ü., Locatelli, M., et al. (2022). Sensitive Determination of Venlafaxine in Urine Samples by Using HPLC-DAD System After Fabric Phase Sorptive Extraction. Cumhuriyet Science Journal, 43(4), 600-605. https://doi.org/10.17776/csj.1182848

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