Structural, electrical, thermal, mechanical properties and micro-hardness in Sn-based Sn-Pb-Al ternary alloys

Canan Alper Billur; Mehmet Arı; Tuncay Karaaslan; Buket Saatçi

doi:10.17776/csj.341093

TR EN

Sn Temelli Sn-Pb-Al Üçlü Alaşımında Yapısal, Elektriksel, Termal, Mekaniksel Özellikler ve Mikrosertlik

Öz

Ötektik Sn-Pb-Al (Sn_61.82Pb_38.10Al_0.08) üçlü alaşımı ve sabit Al konsantrasyonunda Sn-Pb-Al üçlü alaşımının (Sn-[x] wt. % Pb-10 wt. % Al) (x=40, 30, 20 and 10) beş farklı örneğinin yapısal, elektriksel, termal, mekaniksel özelliği ve mikrosertliği araştırıldı. Örneklerin sıcaklığa bağlı olarak elektriksel iletkenliği dört nokta elektriksel iletkenlik tekniği kullanılarak ölçüldü. Örneklerin sıcaklığa bağlı olarak termal iletkenliği elektriksel ölçümlerden elde edilen datalarla birlikte Wiedemann-Franz (W-F) yasasıyla gösterildi. Taramalı elektron mikroskobu(SEM), X ışınları difraktometresi(XRD), EDX ölçümleri, yüzey morfolojisini açığa çıkartmak, kristal yapı, hücre parametreleri, tane boyutları ve kimyasal bileşimini belirlemek için gerçekleştirildi. Çekme testleri alaşımdaki her bir bileşimin tane boyutlarına bağlı olarak en büyük gerilme mukavemetini belirlemek için gerçekleştirildi. Alaşımın herbir bileşimi için mikrosertlik sonuçları Vickers test cihazı kullanılarak bulundu.

Anahtar Kelimeler

References

[1]. Guang-ming X., Bao-mian L., Jian-zhong C., Effect of Heat Treatment on Microstructure and Property of Al-Sn-Pb Bearing Material, J. Iron Steel Res. Int., 2006, 13, 2, 73-76.
[2]. Noskova N.I., Korshunov L.G., Korznikov A.V., Microstructure and tribological properties of Al - Sn, Al - Sn - Pb, AND Sn - Sb - Cu alloys subjected to severe plastic deformation, Met. Sci. Heat Treat., 2008, 50, 11-12, 593-599.
[3]. Noskova N.I., Vil’danova N.F., Filippov YuI., Churbaev R.V., Pereturina I.A., Korshunov L.G., Korznikov A.V., Preparation, deformation, and failure of functional Al-Sn and Al-Sn-Pb nanocrystalline alloys, The Physics of Metals and Metallography, 2006, 102, 646-651.
[4]. Shim J.H., Lee H.N., Ha H.P., Cho Y.W., Yoon E.P., Liquid miscibility gap in the Al-Pb-Sn system, J. Alloys Compd., 2001, 327, 270-274.
[5]. Kittel C. Introduction to Solid State Physics, 8th Ed. John Wiley and Sons, New York, 2005, pp. 156.
[6]. Ari M., Saatçi B., Gündüz M., Meydaneri F., Bozoklu M., Microstructure and Thermo-Electrical Transport Properties Of Cd-Sn Alloys, Mater. Charact., 2008, 59, 624-630.
[7]. Saatçi B., Ari M., Gündüz M., Türktekin S., Meydaneri F., Durmuş S., Özdemir M., Structural and Transport Properties Of Sn-Mg Alloys, Continuum Mech. Thermodyn., 2013, 25,739-748.
[8]. Ocak Y., Aksöz S., Maraşlı N., Keşlioğlu K., Thermal and electrical conductivity of Sn–Ag-In alloys, J. Non-Crystalline Solids., 2010, 356, 1795-1801.

[9]. Aksöz S., Maraşlı N., Thermal and And Electrical Conductivities Of Silver-Indium-Tin Alloys, J. Physics Chem.Solids., 2012, 73, 902-910.
[10]. Ari M., Saatçi B., Gündüz M., Payveren M., S. Durmuş, Thermo-Electrical Characterization of Sn-Zn Alloys, Mater. Charact., 2008, 59, 757-763.
[11]. Saatci B., Ari M., Gündüz M., Meydaneri F., Bozoklu M., Durmus S., Thermal and Electrical Conductivities Of Cd-Zn Alloys, J. Phys. Condens. Matter., 2006, 18, 10643-10653.
[12]. Meydaneri F., Ari M., Saatçi B., Thermo-Electrical Characterization Of Lead-Cadmium (Pb-Cd) Alloys, Accepted Manuscript, Int. J. Phys. Sci., 2012, 7, 48, 6210-6221.
[13]. Cullity B.D.: Elements of X-Ray Diffraction, Inc, third edition, Addison-Wesley Publishing Company, United States of America, 1967. [14]. Callister W.D.: Materials Science and Engineering-An Introduction, John Wiley and Sons, New York, 1997.
[15]. Smits F.M., Measurement the of Sheet Resistivities Four-Point Probe, The Bell sys. Tech. J., 1958, 711-718.
[16]. Ziya A.B., Ohshima K., X-ray diffraction study of the structure and thermal parameters of the ternary Au–Ag–Pd alloys, J. Alloys Compd., 2006,425, 123-128.
[17]. Juˇsk˙enas R., Mockus Z., Kanapeckaite S., Stalnionis G., Survila A., XRD studies of the phase composition of the electrodeposited copper-rich Cu–Sn alloys, Electrochimica Acta. 2006, 52 , 928-935.
[18]. Ortiz A.L., Shaw L., X-ray diffraction analysis of a severely plastically deformed aluminum alloy, Acta Mater., 2004, 52, 2185-2197.
[19]. Shalaby R.M., Effect of silicon addition on mechanical and electrical properties of Sn–Zn based alloys rapidly quenched from melt, Materials Science and Engineering A, 2012, 550, 112-117.
[20]. Shalaby R.M., Effect of silver and indium addition on mechanical properties and indentation creep behavior of rapidly solidified Bi–Sn based lead-free solder alloys, Materials Science and Engineering A, 2013, 560, 86-95.
[21]. Billah Md.M., Shorowordi K.M., Sharif A., Effect of micron size Ni particle addition in Sn–8Zn–3Bi lead-free solder alloy on the microstructure, thermal and mechanical propertiesJ. Alloys Compd., 2014, 585, 32-39.
[22]. Scherrer P., Nachrichten von der Gesellschaft der Wissenschaften zu Göttingen, Mathematisch-Physikalische Klasse, Göttinger Nachrichten Gesell. (1918) 98-100.
[23]. Patterson A.L., The Scherrer Formula for X-Ray Particle Size Determination, Phys. Rev., 1939, 56,978-982.
[24]. Mishra R., Zemanova A., Kroupa A., Flandorfer H., Ipser H., Synthesis and characterization of Sn-rich Ni–Sb–Sn nanosolders, J. Alloys Compd., 2012, 513, 224-229.
[25]. E. Çadırlı, U. Böyük, H. Kaya, N. Maraşlı, S. Aksöz, Y. Ocak, Dependence Of Electrical Resistivity On Temperature And Sn Content In Pb-Sn Solders, J. Elect. Mater., 2011, 40, 2,195-200.
[26]. E. Çadırlı, H. Kaya, The effect of composition on microhardness and determination of electrical and thermal properties in the Sn-Cu alloys, J. Mater. Sci : Materıals In Electronıcs. 2011, 22, 1378-1386.
[27]. Çadirli E., Böyük U., Kaya H., Maraşli N., Determination Of Mechanical, Electrical And Thermal Properties Of The Sn-Bi-Zn Ternary Alloy, J. Non-Crystalline Solids, 2011, 357, 2876-2881.
[28]. Y. Ocak, S. Aksöz, N. Maraşli, K. Keşlioğlu, Dependency Of Thermal And Electrical Conductivity On Temperature And Composition Of Sn In Pb-Sn Alloys, Fluid Phase Equilibria, 2010, 295, 60-67.
[29]. Öztürk E., Aksöz S., Keşlioğlu K., Maraşli N., The Measurement Of Thermal Conductivity Variation With Temperature For Sn-20 Wt.% In Based Lead-Free Ternary Solders Thermochimica Acta, 2013, 554, 63-70.
[30]. Kaygisiz Y., Ocak Y., Aksöz S., Keşlioğlu K., Maraşli N., Thermal Conductivity And Interfacial Energies Of Solid Sn3sb2 In The Sn-Sb Peritectic System, Thermochimica Acta. 2011,520, 25-32.
[31]. Saatçi B., Çimen S., Pamuk H., Gündüz M., The interfacial free energy of solid Sn on the boundary interface with liquid Cd–Sn eutectic solution, J. Phys. Condens. Matter. 2007; 19: 326219 (11pp).
[32]. Aksöz S., Ocak Y., Keşlioğlu K. Maraşlı N., Determination Of Thermo-Electrical Properties In Sn Based Alloys, Met. Mater. Int. 2010, 16, 3, 507-515.
[33]. Saatçi B., Maraşlı N., Gündüz M., Thermal Conductivities Of Solid And Liquid Phases In Pb-Cd And Sn-Zn Binary Eutectic Alloys, Thermochimica Acta, 2007 ; 454 : 128-134.

Details

Primary Language

English

Subjects

-

Journal Section

Research Article

Authors

Canan Alper Billur
Türkiye

Mehmet Arı

Tuncay Karaaslan

Buket Saatçi

Publication Date

December 8, 2017

Submission Date

October 2, 2017

Acceptance Date

October 24, 2017

Published in Issue

Year 1970 Volume: 38 Number: 4

DOI

https://doi.org/10.17776/csj.341093

IZ

https://izlik.org/JA52KB22CT

Cite

RIS / Bibtex

APA

Alper Billur, C., Arı, M., Karaaslan, T., & Saatçi, B. (2017). Structural, electrical, thermal, mechanical properties and micro-hardness in Sn-based Sn-Pb-Al ternary alloys. Cumhuriyet Science Journal, 38(4), 39-51. https://doi.org/10.17776/csj.341093

Structural, electrical, thermal, mechanical properties and micro-hardness in Sn-based Sn-Pb-Al ternary alloys

Sn Temelli Sn-Pb-Al Üçlü Alaşımında Yapısal, Elektriksel, Termal, Mekaniksel Özellikler ve Mikrosertlik

Öz

Anahtar Kelimeler