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A new spectrophotometric study with ortho hydroxy schiff base for the determination of aluminum in drug

Yıl 2020, Cilt: 41 Sayı: 2, 456 - 461, 25.06.2020

Tufan Güray , Dila Ercengiz Ülkü Dilek Uysal

https://doi.org/10.17776/csj.693029

Öz

In this study, a Schiff base called (E)-2-((2- hydroxy -3- methoxy benzylidene)amino)-5- methylphenol (L) was used as a ligand. Spectrophotometric properties of the ligand have been defined and the optimum conditions for determining aluminium by complex by UV-Vis. spectrophotometry. The absorbance of Al(III)-L complex obeys Beer’s law between 1.4 µg mL–1 and 13.5 µg mL–1 for the aluminium in the optimum conditions. Under optimum conditions, the determination of aluminium in Kompensan® drug was done successfully. The LOD and LOQ values of the developed method were 0.01139 μg mL-1 and 0.0345 μg mL-1, respectively for the ligand.

Anahtar Kelimeler

Aluminium Schiff base UV- Vis. spectrophotometry Kompensan®

Destekleyen Kurum

Anadolu Üniversitesi

Proje Numarası

1509F633

Teşekkür

We kindly acknowledge to Anadolu University Scientific Research Projects (No:1509F633) for its support to this study.

Kaynakça

  • [1] Farndon, J. The elements. Aluminum. Benchmark Books, 2001, New York.
  • [2] Nayak, P. Aluminium: impacts and disease. Environmental Research. 89(2) (2002) 101–115.
  • [3] Santarossa, D. G., Talio, M. C. and Fernández, L. P. Aluminium traces determination in biological and water samples using a novel extraction scheme combined with molecular fluorescence. Microchem. J., 129 (2016) 274-280.
  • [4] Minshall, C., Nadal, J. and Exley, C. Aluminium in human sweat. J.Trace Elem. Med. and Bio., 28 (1) (2014) 87-88.
  • [5] Antoine, J. M. R., HooFung, L. A., Grant, C. N. Assessment of the potential health risks associated with the aluminium, arsenic, cadmium and lead content in selected fruits and vegetables grown in Jamaica. Toxicology Reports, 4 (2017) 181 -187.
  • [6] Frankowski, M. Aluminium and Its Complexes in Teas and Fruity Brew Samples, Speciation and Ions Determination by Ion Chromatography and High-Performance Liquid Chromatography–Fluorescence Analytical Methods. Food Analy. Met., 7 (5) (2014) 1109–1117.
  • [7] Kalogria, E., Varvaresou, A., Papageorgiou, S., Protopapa, E., Tsaknis, I., Matikas, A. and Panderi, I. Pre-Column Derivatization HPLC Procedure for the Quantitation of Aluminium Chlorohydrate in Antiperspirant Creams Using Quercetin as Chromogenic Reagent. Chromatographia, 77 (19-20) (2014) 1275-1281.
  • [8] Hydes, D. J. and Liss, P. S. Fluorimetric Method for the Determination of Low Concentrations of Dissolved Aluminium in Natural Waters. Analyst, 101 (1976) 922- 931.
  • [9] Pedrozo-Peñafiel, M.J., Doyle, A., Mendes, L.A.N., Tristão, M.L.B., Saavedra, A. and Aucelio, R.Q. Methods for the determination of silicon and aluminum in fuel oils and in crude oils by X-ray fluorescence spectrometry. Fuel, 243 (2019) 493- 500.
  • [10] Qiong, L., Lirong, W., Danli, X. and Guanghan L. Determination of trace aluminum in foods by stripping voltammetry. Food Chem., 97(1) (2006) 176-180.
  • [11] Ritchie, G.S.P., Posner, A.M., and Ritchie, I.M. The determination of trace levels of aluminum by differential pulse polarography. Anal. Chim. Acta, 117, (1980) 233-239,
  • [12] Eroglu E. I., Gulec, A. and Ayaz A. Determination of aluminium leaching into various baked meats with different types of foils by ICP‐MS. J. Food Process. Preserv., 42 (12) (2018) 1-9.
  • [13] Fairman, B. and Sanz-Medel, A. Flow injection-mini-column technique with ICP-AES detection for the isolation and preconcentration of the fast reactive aluminium fraction in waters. Fresenius J. Anal. Chem., 355 (1996) 757- 762.
  • [14] Huseyinli A.A., Alievaa R., Haciyevaa S. and Guray T. Spectrophotometric determination of aluminium and indium with 2,2',3,4-tetrahydroxy-3',5'-disulphoazobenzene. J. Hazard. Mat., 163 (2-3) (2009) 1001-1007.
  • [15] Guray T., Uysal U.D., Gedikbey T. and Huseyinli A.A. 2,2',3,4-Tetrahydroxy-3'-sulpho-5'-nitroazobenzene for spectrophotometric determination of aluminium in pharmaceutical suspensions and granite. Anal. Chim. Acta, 545 (2005) 107–112.
  • [16] Guray T., Ogretir C., Gedikbey T. and Huseyinli A.A. Synthesis and spectrophotometric determination of acidity constants of 2,3,4,6'-tetrahydroxy-3'-sulfoazobenzene and their use in determination of aluminum. Turk. J. Chem., 35 (2011) 291– 305.
  • [17] Huseyinli A.A. and Aliyeva R.A. A new tetrahydroxyazon SC analytical reagent for the spectrophotometric determination of Al(III), In(III), and Ga(III). Anal. Sci., 17 (2001) 1683– 1685.
  • [18] Ahmed, M.J., Hoque, M.R., Khan, S.H. and Bhattacharjee, S.C. A simple spectrophotometric method for the determination of aluminum in some environmental, biological, soil and pharmaceutical samples using 2-hydroxynaphthaldehydebenzoylhydrazone. Eurasian J. Anal. Chem., 5(1) (2010) 1-15.
  • [19] Saritha, B. and Reddy, T.S. Direct Spectrophotometric determination of Aluminum (III) using 5-Bromo-2-hydroxy-3-methoxybenzaldehyde-P-hydroxybenzoic hydrazine. IOSR J. Applied Chem., 7 (2) (2014) 5-10.
  • [20] Khajehsharifi, H., Solhjoo, A. and Bordbar M. M. Design of an Optical Sensor for Aluminium(III) Determination Based on Immobilization of Eriochrome Cyanine R on a Triacetylcellulose. Iranian J. Anal. Chem., 3 (2) (2016) 145-152.
  • [21] Zhou, T., Huang, Y., Yuan, D., Feng, S., Zhu, Y., Ma, J. A sensitive flow-injection analysis method with iminodiacetate chelation and spectrophotometric detection for on board determination of trace dissolved aluminum in seawater. Analytical Methods, 8(22) (2016) 4473-4481.
  • [22] Lima, L. C., Papai and R., Gaubeur, I. Butan-1-ol as an extractant solvent in dispersive liquid-liquid microextraction in the spectrophotometric determination of aluminium. J. Trace Elements Med. Bio., 50 (2018). 175-181.
  • [23] Oter O., Ertekin K., Kılıncarslan R., Ulusoy M. and Cetinkaya B. Photocharacterization of a novel fluorescent Schiff Base and investigation of its utility as an optical Fe3+ sensor in PVC matrix. Dyes and Pigments, 74(3) (2007) 730-735.
  • [24] Baran N.Y. and Saçak M. Synthesis, characterization and molecular weight monitoring of a novel Schiff base polymer containing phenol group: Thermal stability, conductivity and antimicrobial properties. J. Mole. Struc., 1146 (2017) 104-112.
  • [25] Ejidike I.P. and Ajibade P.A. Transition metal complexes of symmetrical and asymmetrical Schiff bases as antibacterial, antifungal, antioxidant, and anticancer agents: Progress and prospects. Rev. Inorg. Chem., 35(4) (2015) 191–224.
  • [26] Napier I., Ponka P., Richardson Des R., Iron trafficking in the mitochondrion: novel pathways revealed by disease, Blood,105(5) (2005) 1867-1874.
  • [27] Percino M.J., Cerón M., Castro M.E., R Ramírez R., Soriano G. and Chapela V.M. (E)-2-[(2-hydroxybenzylidene)amino]phenylarsonic acid Schiff base: Synthesis, characterization and theoretical studies. J. Mol. Struc., 1081 (2015) 193-200.
  • [28] Al-Shemary R.K., Al-khazraji A.M.A., Niseaf A.N. Preparation, spectroscopic study of Schiff base ligand complexes with some metal ions and Evaluation of antibacterial activity. The Pharma Innovat. J. 5(1) (2016) 81-86.
  • [29] Uysal U.D., Güray T., Berber H., Ercengiz D., Aydoğdu A., 2018, Synthesis of Certain Schiff Bases Formed Substituted 2-Aminophenol and Substituted Hydroxy Benzaldehyde, Spectroscopic Study and Investigation of Their Applications on Metal Determination in Different Samples, Anadolu University Scientific Research Projects (No:1509F633).
  • [30] The United States Pharmacopeia-National Formulary, United States Pharmacopeial Convention, Rockville, MD, 1999.
  • [31] Suresha S., Silwadi M.F. and Syed A.A. Sensitive and selective spectrophotometric determination of Hg(II), Ni(II), Cu(II) and Co(II) using iminodibenzyl and 3- chloroiminodibenzyl as new reagents and their applications to industrial effluents and soil samples, Int. J. Environ. Anal. Chem., 82 (2002) 275-289.
  • [32] Khopkar S.M., Basic Concepts of Analytical Chemistry, 3rd edition ed., New Age Science, 2008, pp. 211-240.

Yıl 2020, Cilt: 41 Sayı: 2, 456 - 461, 25.06.2020

Tufan Güray , Dila Ercengiz Ülkü Dilek Uysal

https://doi.org/10.17776/csj.693029

Öz

Proje Numarası

1509F633

Kaynakça

  • [1] Farndon, J. The elements. Aluminum. Benchmark Books, 2001, New York.
  • [2] Nayak, P. Aluminium: impacts and disease. Environmental Research. 89(2) (2002) 101–115.
  • [3] Santarossa, D. G., Talio, M. C. and Fernández, L. P. Aluminium traces determination in biological and water samples using a novel extraction scheme combined with molecular fluorescence. Microchem. J., 129 (2016) 274-280.
  • [4] Minshall, C., Nadal, J. and Exley, C. Aluminium in human sweat. J.Trace Elem. Med. and Bio., 28 (1) (2014) 87-88.
  • [5] Antoine, J. M. R., HooFung, L. A., Grant, C. N. Assessment of the potential health risks associated with the aluminium, arsenic, cadmium and lead content in selected fruits and vegetables grown in Jamaica. Toxicology Reports, 4 (2017) 181 -187.
  • [6] Frankowski, M. Aluminium and Its Complexes in Teas and Fruity Brew Samples, Speciation and Ions Determination by Ion Chromatography and High-Performance Liquid Chromatography–Fluorescence Analytical Methods. Food Analy. Met., 7 (5) (2014) 1109–1117.
  • [7] Kalogria, E., Varvaresou, A., Papageorgiou, S., Protopapa, E., Tsaknis, I., Matikas, A. and Panderi, I. Pre-Column Derivatization HPLC Procedure for the Quantitation of Aluminium Chlorohydrate in Antiperspirant Creams Using Quercetin as Chromogenic Reagent. Chromatographia, 77 (19-20) (2014) 1275-1281.
  • [8] Hydes, D. J. and Liss, P. S. Fluorimetric Method for the Determination of Low Concentrations of Dissolved Aluminium in Natural Waters. Analyst, 101 (1976) 922- 931.
  • [9] Pedrozo-Peñafiel, M.J., Doyle, A., Mendes, L.A.N., Tristão, M.L.B., Saavedra, A. and Aucelio, R.Q. Methods for the determination of silicon and aluminum in fuel oils and in crude oils by X-ray fluorescence spectrometry. Fuel, 243 (2019) 493- 500.
  • [10] Qiong, L., Lirong, W., Danli, X. and Guanghan L. Determination of trace aluminum in foods by stripping voltammetry. Food Chem., 97(1) (2006) 176-180.
  • [11] Ritchie, G.S.P., Posner, A.M., and Ritchie, I.M. The determination of trace levels of aluminum by differential pulse polarography. Anal. Chim. Acta, 117, (1980) 233-239,
  • [12] Eroglu E. I., Gulec, A. and Ayaz A. Determination of aluminium leaching into various baked meats with different types of foils by ICP‐MS. J. Food Process. Preserv., 42 (12) (2018) 1-9.
  • [13] Fairman, B. and Sanz-Medel, A. Flow injection-mini-column technique with ICP-AES detection for the isolation and preconcentration of the fast reactive aluminium fraction in waters. Fresenius J. Anal. Chem., 355 (1996) 757- 762.
  • [14] Huseyinli A.A., Alievaa R., Haciyevaa S. and Guray T. Spectrophotometric determination of aluminium and indium with 2,2',3,4-tetrahydroxy-3',5'-disulphoazobenzene. J. Hazard. Mat., 163 (2-3) (2009) 1001-1007.
  • [15] Guray T., Uysal U.D., Gedikbey T. and Huseyinli A.A. 2,2',3,4-Tetrahydroxy-3'-sulpho-5'-nitroazobenzene for spectrophotometric determination of aluminium in pharmaceutical suspensions and granite. Anal. Chim. Acta, 545 (2005) 107–112.
  • [16] Guray T., Ogretir C., Gedikbey T. and Huseyinli A.A. Synthesis and spectrophotometric determination of acidity constants of 2,3,4,6'-tetrahydroxy-3'-sulfoazobenzene and their use in determination of aluminum. Turk. J. Chem., 35 (2011) 291– 305.
  • [17] Huseyinli A.A. and Aliyeva R.A. A new tetrahydroxyazon SC analytical reagent for the spectrophotometric determination of Al(III), In(III), and Ga(III). Anal. Sci., 17 (2001) 1683– 1685.
  • [18] Ahmed, M.J., Hoque, M.R., Khan, S.H. and Bhattacharjee, S.C. A simple spectrophotometric method for the determination of aluminum in some environmental, biological, soil and pharmaceutical samples using 2-hydroxynaphthaldehydebenzoylhydrazone. Eurasian J. Anal. Chem., 5(1) (2010) 1-15.
  • [19] Saritha, B. and Reddy, T.S. Direct Spectrophotometric determination of Aluminum (III) using 5-Bromo-2-hydroxy-3-methoxybenzaldehyde-P-hydroxybenzoic hydrazine. IOSR J. Applied Chem., 7 (2) (2014) 5-10.
  • [20] Khajehsharifi, H., Solhjoo, A. and Bordbar M. M. Design of an Optical Sensor for Aluminium(III) Determination Based on Immobilization of Eriochrome Cyanine R on a Triacetylcellulose. Iranian J. Anal. Chem., 3 (2) (2016) 145-152.
  • [21] Zhou, T., Huang, Y., Yuan, D., Feng, S., Zhu, Y., Ma, J. A sensitive flow-injection analysis method with iminodiacetate chelation and spectrophotometric detection for on board determination of trace dissolved aluminum in seawater. Analytical Methods, 8(22) (2016) 4473-4481.
  • [22] Lima, L. C., Papai and R., Gaubeur, I. Butan-1-ol as an extractant solvent in dispersive liquid-liquid microextraction in the spectrophotometric determination of aluminium. J. Trace Elements Med. Bio., 50 (2018). 175-181.
  • [23] Oter O., Ertekin K., Kılıncarslan R., Ulusoy M. and Cetinkaya B. Photocharacterization of a novel fluorescent Schiff Base and investigation of its utility as an optical Fe3+ sensor in PVC matrix. Dyes and Pigments, 74(3) (2007) 730-735.
  • [24] Baran N.Y. and Saçak M. Synthesis, characterization and molecular weight monitoring of a novel Schiff base polymer containing phenol group: Thermal stability, conductivity and antimicrobial properties. J. Mole. Struc., 1146 (2017) 104-112.
  • [25] Ejidike I.P. and Ajibade P.A. Transition metal complexes of symmetrical and asymmetrical Schiff bases as antibacterial, antifungal, antioxidant, and anticancer agents: Progress and prospects. Rev. Inorg. Chem., 35(4) (2015) 191–224.
  • [26] Napier I., Ponka P., Richardson Des R., Iron trafficking in the mitochondrion: novel pathways revealed by disease, Blood,105(5) (2005) 1867-1874.
  • [27] Percino M.J., Cerón M., Castro M.E., R Ramírez R., Soriano G. and Chapela V.M. (E)-2-[(2-hydroxybenzylidene)amino]phenylarsonic acid Schiff base: Synthesis, characterization and theoretical studies. J. Mol. Struc., 1081 (2015) 193-200.
  • [28] Al-Shemary R.K., Al-khazraji A.M.A., Niseaf A.N. Preparation, spectroscopic study of Schiff base ligand complexes with some metal ions and Evaluation of antibacterial activity. The Pharma Innovat. J. 5(1) (2016) 81-86.
  • [29] Uysal U.D., Güray T., Berber H., Ercengiz D., Aydoğdu A., 2018, Synthesis of Certain Schiff Bases Formed Substituted 2-Aminophenol and Substituted Hydroxy Benzaldehyde, Spectroscopic Study and Investigation of Their Applications on Metal Determination in Different Samples, Anadolu University Scientific Research Projects (No:1509F633).
  • [30] The United States Pharmacopeia-National Formulary, United States Pharmacopeial Convention, Rockville, MD, 1999.
  • [31] Suresha S., Silwadi M.F. and Syed A.A. Sensitive and selective spectrophotometric determination of Hg(II), Ni(II), Cu(II) and Co(II) using iminodibenzyl and 3- chloroiminodibenzyl as new reagents and their applications to industrial effluents and soil samples, Int. J. Environ. Anal. Chem., 82 (2002) 275-289.
  • [32] Khopkar S.M., Basic Concepts of Analytical Chemistry, 3rd edition ed., New Age Science, 2008, pp. 211-240.
Toplam 32 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Bölüm Natural Sciences
Yazarlar

Tufan Güray 0000-0002-7509-7260

Dila Ercengiz 0000-0001-7642-633X

Ülkü Dilek Uysal 0000-0003-1572-9753

Proje Numarası 1509F633
Yayımlanma Tarihi 25 Haziran 2020
Gönderilme Tarihi 23 Şubat 2020
Kabul Tarihi 5 Haziran 2020
Yayımlandığı Sayı Yıl 2020Cilt: 41 Sayı: 2

Kaynak Göster

APA Güray, T., Ercengiz, D., & Uysal, Ü. D. (2020). A new spectrophotometric study with ortho hydroxy schiff base for the determination of aluminum in drug. Cumhuriyet Science Journal, 41(2), 456-461. https://doi.org/10.17776/csj.693029