A new spectrophotometric study with ortho hydroxy schiff base for the determination of aluminum in drug
Yıl 2020,
, 456 - 461, 25.06.2020
Tufan Güray
,
Dila Ercengiz
Ülkü Dilek Uysal
Öz
In this study, a Schiff base called (E)-2-((2- hydroxy -3- methoxy benzylidene)amino)-5- methylphenol (L) was used as a ligand. Spectrophotometric properties of the ligand have been defined and the optimum conditions for determining aluminium by complex by UV-Vis. spectrophotometry. The absorbance of Al(III)-L complex obeys Beer’s law between 1.4 µg mL–1 and 13.5 µg mL–1 for the aluminium in the optimum conditions. Under optimum conditions, the determination of aluminium in Kompensan® drug was done successfully. The LOD and LOQ values of the developed method were 0.01139 μg mL-1 and 0.0345 μg mL-1, respectively for the ligand.
Destekleyen Kurum
Anadolu Üniversitesi
Teşekkür
We kindly acknowledge to Anadolu University Scientific Research Projects (No:1509F633) for its support to this study.
Kaynakça
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Yıl 2020,
, 456 - 461, 25.06.2020
Tufan Güray
,
Dila Ercengiz
Ülkü Dilek Uysal
Kaynakça
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- [2] Nayak, P. Aluminium: impacts and disease. Environmental Research. 89(2) (2002) 101–115.
- [3] Santarossa, D. G., Talio, M. C. and Fernández, L. P. Aluminium traces determination in biological and water samples using a novel extraction scheme combined with molecular fluorescence. Microchem. J., 129 (2016) 274-280.
- [4] Minshall, C., Nadal, J. and Exley, C. Aluminium in human sweat. J.Trace Elem. Med. and Bio., 28 (1) (2014) 87-88.
- [5] Antoine, J. M. R., HooFung, L. A., Grant, C. N. Assessment of the potential health risks associated with the aluminium, arsenic, cadmium and lead content in selected fruits and vegetables grown in Jamaica. Toxicology Reports, 4 (2017) 181 -187.
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- [19] Saritha, B. and Reddy, T.S. Direct Spectrophotometric determination of Aluminum (III) using 5-Bromo-2-hydroxy-3-methoxybenzaldehyde-P-hydroxybenzoic hydrazine. IOSR J. Applied Chem., 7 (2) (2014) 5-10.
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- [22] Lima, L. C., Papai and R., Gaubeur, I. Butan-1-ol as an extractant solvent in dispersive liquid-liquid microextraction in the spectrophotometric determination of aluminium. J. Trace Elements Med. Bio., 50 (2018). 175-181.
- [23] Oter O., Ertekin K., Kılıncarslan R., Ulusoy M. and Cetinkaya B. Photocharacterization of a novel fluorescent Schiff Base and investigation of its utility as an optical Fe3+ sensor in PVC matrix. Dyes and Pigments, 74(3) (2007) 730-735.
- [24] Baran N.Y. and Saçak M. Synthesis, characterization and molecular weight monitoring of a novel Schiff base polymer containing phenol group: Thermal stability, conductivity and antimicrobial properties. J. Mole. Struc., 1146 (2017) 104-112.
- [25] Ejidike I.P. and Ajibade P.A. Transition metal complexes of symmetrical and asymmetrical Schiff bases as antibacterial, antifungal, antioxidant, and anticancer agents: Progress and prospects. Rev. Inorg. Chem., 35(4) (2015) 191–224.
- [26] Napier I., Ponka P., Richardson Des R., Iron trafficking in the mitochondrion: novel pathways revealed by disease, Blood,105(5) (2005) 1867-1874.
- [27] Percino M.J., Cerón M., Castro M.E., R Ramírez R., Soriano G. and Chapela V.M. (E)-2-[(2-hydroxybenzylidene)amino]phenylarsonic acid Schiff base: Synthesis, characterization and theoretical studies. J. Mol. Struc., 1081 (2015) 193-200.
- [28] Al-Shemary R.K., Al-khazraji A.M.A., Niseaf A.N. Preparation, spectroscopic study of Schiff base ligand complexes with some metal ions and Evaluation of antibacterial activity. The Pharma Innovat. J. 5(1) (2016) 81-86.
- [29] Uysal U.D., Güray T., Berber H., Ercengiz D., Aydoğdu A., 2018, Synthesis of Certain Schiff Bases Formed Substituted 2-Aminophenol and Substituted Hydroxy Benzaldehyde, Spectroscopic Study and Investigation of Their Applications on Metal Determination in Different Samples, Anadolu University Scientific Research Projects (No:1509F633).
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chloroiminodibenzyl as new reagents and their applications to industrial effluents and soil samples, Int. J. Environ. Anal. Chem., 82 (2002) 275-289.
- [32] Khopkar S.M., Basic Concepts of Analytical Chemistry, 3rd edition ed., New Age Science, 2008, pp. 211-240.