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Year 2021, Volume: 5 Issue: 4, 326 - 335, 31.12.2021

Hafize Fidan Stanko Stankov Nadezhda Petkova Bozhidar Bozadzhiev Milen Dimov Lazar Lazarov Apostol Simitchiev Albena Stoyanova

https://doi.org/10.30521/jes.962474

Abstract

Project Number

КP-06-H36/14

References

  • [1] Scatolino, M, Neto, L, Protaslo, T, Carneiro, A, Andrade, C, Guimaraes J, Mended, L. Options for Generation of Sustainable Energy: Production of Pellets Based on Combinations between Lignocellulose Biomasses. Waste and Biomass Valorization 2017; 9: 479-489, DOI : 10.1007/s12649-017-0010-2.
  • [2] Hmaied, M, Bouafif, H, Magdouli, S, Braghiroli, FL, Koubaa, A. Effect of Forest Biomass Pretreatment on Essential Oil Yield and Properties. Forests 2019; 10: 1042, DOI: 10.3390/f10111042.
  • [3] Bilandzija, N, Voca, N, Jelcic, B, Jurisic, V, Martin, A, Grubor, M, Kricka, T. Evaluation of Croatian agricultural solid biomass energy potential. Renewable and Sustainable Energy Reviews 2018; 93: 225-230.
  • [4] Móricz, N, Garamszegi, B, Rasztovits, E, Bidló, A, Horváth, A, Jagicza, A, Illés, G, Vekerdy, Z, Somogyi, Z, Gálos, B. Recent Drought-Induced Vitality Decline of Black Pine (Pinus nigra Arn.) in South-West Hungary—Is This Drought-Resistant Species under Threat by Climate Change? Forests 2018; 9: 414, DOI : 10.3390/f9070414.
  • [5] Sherwood, J. The Significance of Biomass in a Circular Economy. Bioresource Technology 2020; 300, 122755, DOI: 10.1016/j.biortech.2020.122755.
  • [6] Ferreira, PT, Ferreira, ME, Teixeira, JC. Analysis of Industrial Waste in Wood Pellets and Co-combustion Products. Waste and Biomass Valorization 2014; 5: 637-650, DOI: https://doi.org/10.1007/s12649-013-9271-6.
  • [7] Holubcik, M, Jachniak, E, Jandacka J. Utilization of materials from agriculture to produce pellets. Archives of Waste Management and Environmental Protection 2015; 17(2): 1-10.
  • [8] Rabacal, M, Fernandez, U, Costa, M. Combustion and Emission Characteristics of a Domestic Boiler Fired with Pellets of Pine, Industrial Wood Wastes and Peach Stones. Renewable Energy 2013; 51: 220-226.
  • [9] Lazarov, L, Bozadzhiev, B, Simitchiev, A, Stoyanova, A. Characteristics of Biomass from Distilled Greek Juniper Needles. Youth Forum Science, Technology, Innovation, Business, 28 – 29 May 2020, Plovdiv, Bulgaria, pp. 42-47.
  • [10] Georgiev, E, Stoyanova, А. A guide for the specialist in the aromatic industry. A Guide for the Specialist in the Aromatic Industry Cultivation (in Bulgarian), Plovdiv, UFT Publ. House, 2006, pp. 51-68.
  • [11] Sabeva, G, Tzvetkov, N, Boycheva, S, Gadzhanov, P, Stankov, N. Изследвания за определяне на гориво- техническите характеристики на продукти от растителна биомаса [Studies to Determine the Fuel and Technical Characteristics of Plant Biomass Products] Science Conference EFM (Sozopol) 2012, pp. 63-70. [in Bulgarian].
  • [12] Stoyanova, M, Velichkova, G, Varbanova, М, Stoykov, R. Energy from Ligneous Biomass. Management and Sustainable Development 2014; 46( 3): 76-81.
  • [13] Pantaleo, A, Villarini, M, Colantoni, A, Carlini, M, Santoro, F, Hamedani, SR. Techno-Economic Modeling of Biomass Pellet Routes: Feasibility in Italy. Energies 2020; 13: 1636, DOI:10.3390/en13071636.
  • [14] Balinova, A, Diakov, G. On improved apparatus for microdistillation of rose flowers. Plant Science 1974; 11: 77-85.
  • [15] AOAC. Method 930.05. Ash of plants. Official Methods of Analysis (Horwitz, W. & Latimer Jr., G.W., Eds.). Gaithersburg, MD, USA: AOAC International, 2005.
  • [16] Lichtenhaler, H, Wellbum, A. Determination of Total Carotenoids and Chlorophylls a and b of Leaf in Different Solvent. Biochemical Society Transactions 1983; 11: 591-592.
  • [17] Lichtenthaler, H, Buschmann, C. Extraction of Phytosynthetic Tissues: Chlorophylls and Carotenoids. Current Protocols in Food Analytical. Chemistry 2001; 1: F4.2.1-F4.2.6.
  • [18] Dubois, M, Gilles, K, Hamilton, J, Rebers, P, Smith, F. Colorimetric method for determination of sugars and related substances. Analytical Chemistry 1956; 28(3): 350-356.
  • [19] Hadjikinova, R, Petkova, N, Hadjikinov, D, Denev, P, Hrusavov, D. Development and validation of hplc-rid method for determination of sugars and polyols. Journal of Pharmaceutical Sciences and Research 2017; 9: 1263-1269.
  • [20] Brendel O, Iannetta, P, Stewart, D. A rapid and simple method to isolate pure α-cellulose. Phytochemical Analysis 2000; 11: 7-10.
  • [21] Jewiartz, M, Wrobel, M, Mudruk, K, Szufa, S. Impact of the Drying Temperature and Grinding Technique on Biomass Grindability. Energies 2020; 13: 3392; DOI:10.3390/en13133392.
  • [22] Anukam, AI, Berghel, J, Famewo, EB, Frodeson, S. Improving the Understanding of the Bonding Mechanism of Primary Components of Biomass Pellets through the Use of Advanced Analytical Instruments. Journal of Wood Chemical Technology 2020; 40: 15-32.
  • [23] Kruszelnicka, W, Kasner, R, Bałdowska-Witos, P, Flizikowski, J, Tomporowski, A. The Integrated Energy Consumption Index for Energy Biomass Grinding Technology Assessment. Energies 2020; 13: 1417.
  • [24] Lun, LW, Gunny, AAN, Kasim, FH, Arbain, D. Fourier Transform Infrared Spectroscopy (FTIR) Analysis of Paddy Straw Pulp Treated using Deep Eutectic Solvent. In: AIP Conference Proceedings 2017, ADVANCED MATERIALS ENGINEERING AND TECHNOLOGY V: International Conference on Advanced Material Engineering and Technology; 2016: Published by the American Institute of Physics 1835(1):020049, pp. 020049-1-020049-4.
  • [25] Paul, R, Voevodin, AA, Zemlyanov, D, Roy, AK, Fisher, TS. Microwave-assisted Surface Synthesis of a Boron-carbon-nitrogen Foam and its Desorption Enthalpy. Advanced Functional Materials 2012; 22(17): 3682-3690.
  • [26] Paul, R, Etacheri, V, Pol, VG, Hu, J, Fisher, TS. Highly Porous Three-dimensional Carbon Nanotube Foam as a Freestanding Anode for a Lithium-ion Battery. RSC Advances 2016; 6(83): 79734-79744.
  • [27] Szufa, S, Wielgosinski, G, Piersa, P, Czerwinska, J, Dzikuc, M, Adrian, Ł, Lewandowska, W, Marczak, M. Torrefaction of Straw from Oats and Maize for Use as a Fuel and Additive to Organic Fertilizers—TGA Analysis, Kinetics as Products for Agricultural Purposes. Energies 2020; 13: 2064.
  • [28] Wróbel, M, Jewiarz, M, Mudryk, K, Knapczyk, A. Influence of Raw Material Drying Temperature on the Scots Pine (Pinus sylvestris L.) Biomass Agglomeration Process—A Preliminary Study. Energies 2020; 13: 1809.
  • [29] Nunez, L, Maria's, J, Catalao J. Energy Recovery from Cork Industrial Waste: Production and Characterisation of Cork Pellets. Fuel 2013; 113: 24-30.
  • [30] Deligöz, A, Bayar, E, Genç, M, Karatepe, Y, Kırdar, E, Cankara, FG. Seasonal and needle age-related variations in the biochemical characteristics of Pinus nigra subsp. pallasiana (Lamb.) Holmboe. Journal оf Forest Science 2018; 64: 379-386.
  • [31] Mandre, M, Tullus, H, Klõšeiko, J. Partitioning of carbohydrates and biomass of needles in Scots pine Canopy". Zeitschrift für Naturforschung C 2002; 57(3-4): 296-302.
  • [32] Donohoe, BS, Decker, SR, Tucker, MP, Himmel, ME, Vinzant, TB. Visualizing lignin coalescence and migration through maize cell walls following thermochemical pretreatment. Biotechnology and Bioengineering 2008; 101: 913-925.
  • [33] Yingfu, Z, Songping, Z, Shida, M, Zhiguo, S, Ping, W. Temperature Sensitivity of Cellulase Adsorption on Lignin and its Impact on Enzymatic Hydrolysis of Lignocellulosic Biomass. Journal of Biotechnology 2013; 166: 135-143.

Bio-energy characteristics of black pine (Pinus nigra Arn.) hydrodistillation waste products

Year 2021, Volume: 5 Issue: 4, 326 - 335, 31.12.2021

Hafize Fidan Stanko Stankov Nadezhda Petkova Bozhidar Bozadzhiev Milen Dimov Lazar Lazarov Apostol Simitchiev Albena Stoyanova

https://doi.org/10.30521/jes.962474

Abstract

The present study aimed to investigate the physicochemical and energy characteristics of Pinus nigra Arn. (Pinaceae family) coniferous biomass used after the production of essential oil. The biomass, comprised of needles and needles with twigs, was milled and subjected to sieve analysis, thus producing three groups of particle fractions (between 384 and 413 μm). The infrared spectrum was recorded as 4000–400 сm–1. The results from the study revealed significant differences in the phytochemical composition. Particle fractions were characterized in terms of moisture content (7.10-7.95%), ash (1.96-2.89%), cellulose (21.30-29.20%), total chlorophyll (225.54-896.04 μg/g), total carotenoids (23.52-145.43 μg/g), and polysaccharides (0.14-2.06%). The basic energy indices used in the assessment of biomass potential as conditional fuel were calculated as follows: calorific value (16748.79-16877.86 kJ/kg), the density of wood biomass (390.99-421.17 kg/m3), and heat equivalent (0.224-0.243 J/m3).

Keywords

Bio-energy Renewable Pellets Pinus nigra Waste products

Supporting Institution

National Science Fund of Bulgaria

Project Number

КP-06-H36/14

Thanks

The authors acknowledge the support by the National Science Fund of Bulgaria, project No КP-06-H36/14.

References

  • [1] Scatolino, M, Neto, L, Protaslo, T, Carneiro, A, Andrade, C, Guimaraes J, Mended, L. Options for Generation of Sustainable Energy: Production of Pellets Based on Combinations between Lignocellulose Biomasses. Waste and Biomass Valorization 2017; 9: 479-489, DOI : 10.1007/s12649-017-0010-2.
  • [2] Hmaied, M, Bouafif, H, Magdouli, S, Braghiroli, FL, Koubaa, A. Effect of Forest Biomass Pretreatment on Essential Oil Yield and Properties. Forests 2019; 10: 1042, DOI: 10.3390/f10111042.
  • [3] Bilandzija, N, Voca, N, Jelcic, B, Jurisic, V, Martin, A, Grubor, M, Kricka, T. Evaluation of Croatian agricultural solid biomass energy potential. Renewable and Sustainable Energy Reviews 2018; 93: 225-230.
  • [4] Móricz, N, Garamszegi, B, Rasztovits, E, Bidló, A, Horváth, A, Jagicza, A, Illés, G, Vekerdy, Z, Somogyi, Z, Gálos, B. Recent Drought-Induced Vitality Decline of Black Pine (Pinus nigra Arn.) in South-West Hungary—Is This Drought-Resistant Species under Threat by Climate Change? Forests 2018; 9: 414, DOI : 10.3390/f9070414.
  • [5] Sherwood, J. The Significance of Biomass in a Circular Economy. Bioresource Technology 2020; 300, 122755, DOI: 10.1016/j.biortech.2020.122755.
  • [6] Ferreira, PT, Ferreira, ME, Teixeira, JC. Analysis of Industrial Waste in Wood Pellets and Co-combustion Products. Waste and Biomass Valorization 2014; 5: 637-650, DOI: https://doi.org/10.1007/s12649-013-9271-6.
  • [7] Holubcik, M, Jachniak, E, Jandacka J. Utilization of materials from agriculture to produce pellets. Archives of Waste Management and Environmental Protection 2015; 17(2): 1-10.
  • [8] Rabacal, M, Fernandez, U, Costa, M. Combustion and Emission Characteristics of a Domestic Boiler Fired with Pellets of Pine, Industrial Wood Wastes and Peach Stones. Renewable Energy 2013; 51: 220-226.
  • [9] Lazarov, L, Bozadzhiev, B, Simitchiev, A, Stoyanova, A. Characteristics of Biomass from Distilled Greek Juniper Needles. Youth Forum Science, Technology, Innovation, Business, 28 – 29 May 2020, Plovdiv, Bulgaria, pp. 42-47.
  • [10] Georgiev, E, Stoyanova, А. A guide for the specialist in the aromatic industry. A Guide for the Specialist in the Aromatic Industry Cultivation (in Bulgarian), Plovdiv, UFT Publ. House, 2006, pp. 51-68.
  • [11] Sabeva, G, Tzvetkov, N, Boycheva, S, Gadzhanov, P, Stankov, N. Изследвания за определяне на гориво- техническите характеристики на продукти от растителна биомаса [Studies to Determine the Fuel and Technical Characteristics of Plant Biomass Products] Science Conference EFM (Sozopol) 2012, pp. 63-70. [in Bulgarian].
  • [12] Stoyanova, M, Velichkova, G, Varbanova, М, Stoykov, R. Energy from Ligneous Biomass. Management and Sustainable Development 2014; 46( 3): 76-81.
  • [13] Pantaleo, A, Villarini, M, Colantoni, A, Carlini, M, Santoro, F, Hamedani, SR. Techno-Economic Modeling of Biomass Pellet Routes: Feasibility in Italy. Energies 2020; 13: 1636, DOI:10.3390/en13071636.
  • [14] Balinova, A, Diakov, G. On improved apparatus for microdistillation of rose flowers. Plant Science 1974; 11: 77-85.
  • [15] AOAC. Method 930.05. Ash of plants. Official Methods of Analysis (Horwitz, W. & Latimer Jr., G.W., Eds.). Gaithersburg, MD, USA: AOAC International, 2005.
  • [16] Lichtenhaler, H, Wellbum, A. Determination of Total Carotenoids and Chlorophylls a and b of Leaf in Different Solvent. Biochemical Society Transactions 1983; 11: 591-592.
  • [17] Lichtenthaler, H, Buschmann, C. Extraction of Phytosynthetic Tissues: Chlorophylls and Carotenoids. Current Protocols in Food Analytical. Chemistry 2001; 1: F4.2.1-F4.2.6.
  • [18] Dubois, M, Gilles, K, Hamilton, J, Rebers, P, Smith, F. Colorimetric method for determination of sugars and related substances. Analytical Chemistry 1956; 28(3): 350-356.
  • [19] Hadjikinova, R, Petkova, N, Hadjikinov, D, Denev, P, Hrusavov, D. Development and validation of hplc-rid method for determination of sugars and polyols. Journal of Pharmaceutical Sciences and Research 2017; 9: 1263-1269.
  • [20] Brendel O, Iannetta, P, Stewart, D. A rapid and simple method to isolate pure α-cellulose. Phytochemical Analysis 2000; 11: 7-10.
  • [21] Jewiartz, M, Wrobel, M, Mudruk, K, Szufa, S. Impact of the Drying Temperature and Grinding Technique on Biomass Grindability. Energies 2020; 13: 3392; DOI:10.3390/en13133392.
  • [22] Anukam, AI, Berghel, J, Famewo, EB, Frodeson, S. Improving the Understanding of the Bonding Mechanism of Primary Components of Biomass Pellets through the Use of Advanced Analytical Instruments. Journal of Wood Chemical Technology 2020; 40: 15-32.
  • [23] Kruszelnicka, W, Kasner, R, Bałdowska-Witos, P, Flizikowski, J, Tomporowski, A. The Integrated Energy Consumption Index for Energy Biomass Grinding Technology Assessment. Energies 2020; 13: 1417.
  • [24] Lun, LW, Gunny, AAN, Kasim, FH, Arbain, D. Fourier Transform Infrared Spectroscopy (FTIR) Analysis of Paddy Straw Pulp Treated using Deep Eutectic Solvent. In: AIP Conference Proceedings 2017, ADVANCED MATERIALS ENGINEERING AND TECHNOLOGY V: International Conference on Advanced Material Engineering and Technology; 2016: Published by the American Institute of Physics 1835(1):020049, pp. 020049-1-020049-4.
  • [25] Paul, R, Voevodin, AA, Zemlyanov, D, Roy, AK, Fisher, TS. Microwave-assisted Surface Synthesis of a Boron-carbon-nitrogen Foam and its Desorption Enthalpy. Advanced Functional Materials 2012; 22(17): 3682-3690.
  • [26] Paul, R, Etacheri, V, Pol, VG, Hu, J, Fisher, TS. Highly Porous Three-dimensional Carbon Nanotube Foam as a Freestanding Anode for a Lithium-ion Battery. RSC Advances 2016; 6(83): 79734-79744.
  • [27] Szufa, S, Wielgosinski, G, Piersa, P, Czerwinska, J, Dzikuc, M, Adrian, Ł, Lewandowska, W, Marczak, M. Torrefaction of Straw from Oats and Maize for Use as a Fuel and Additive to Organic Fertilizers—TGA Analysis, Kinetics as Products for Agricultural Purposes. Energies 2020; 13: 2064.
  • [28] Wróbel, M, Jewiarz, M, Mudryk, K, Knapczyk, A. Influence of Raw Material Drying Temperature on the Scots Pine (Pinus sylvestris L.) Biomass Agglomeration Process—A Preliminary Study. Energies 2020; 13: 1809.
  • [29] Nunez, L, Maria's, J, Catalao J. Energy Recovery from Cork Industrial Waste: Production and Characterisation of Cork Pellets. Fuel 2013; 113: 24-30.
  • [30] Deligöz, A, Bayar, E, Genç, M, Karatepe, Y, Kırdar, E, Cankara, FG. Seasonal and needle age-related variations in the biochemical characteristics of Pinus nigra subsp. pallasiana (Lamb.) Holmboe. Journal оf Forest Science 2018; 64: 379-386.
  • [31] Mandre, M, Tullus, H, Klõšeiko, J. Partitioning of carbohydrates and biomass of needles in Scots pine Canopy". Zeitschrift für Naturforschung C 2002; 57(3-4): 296-302.
  • [32] Donohoe, BS, Decker, SR, Tucker, MP, Himmel, ME, Vinzant, TB. Visualizing lignin coalescence and migration through maize cell walls following thermochemical pretreatment. Biotechnology and Bioengineering 2008; 101: 913-925.
  • [33] Yingfu, Z, Songping, Z, Shida, M, Zhiguo, S, Ping, W. Temperature Sensitivity of Cellulase Adsorption on Lignin and its Impact on Enzymatic Hydrolysis of Lignocellulosic Biomass. Journal of Biotechnology 2013; 166: 135-143.
There are 33 citations in total.

Details

Primary Language English
Subjects Material Production Technologies
Journal Section Research Articles
Authors

Hafize Fidan 0000-0002-3373-5949

Stanko Stankov 0000-0003-2332-1782

Nadezhda Petkova 0000-0002-5870-9157

Bozhidar Bozadzhiev 0000-0003-4200-140X

Milen Dimov This is me 0000-0002-8339-3932

Lazar Lazarov 0000-0002-6071-7949

Apostol Simitchiev 0000-0002-2330-8572

Albena Stoyanova 0000-0001-7140-7826

Project Number КP-06-H36/14
Publication Date December 31, 2021
Acceptance Date October 25, 2021
Published in Issue Year 2021 Volume: 5 Issue: 4

Cite

Vancouver Fidan H, Stankov S, Petkova N, Bozadzhiev B, Dimov M, Lazarov L, Simitchiev A, Stoyanova A. Bio-energy characteristics of black pine (Pinus nigra Arn.) hydrodistillation waste products. JES. 2021;5(4):326-35.
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