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Alkilditiyokarbamat Tuzlarının 1,3-Dikloroaseton ile Reaksiyonları

Year 2016, Volume: 6 Issue: 1, 44 - 51, 30.06.2016

Cumhur Kırılmış Esra Barım

Abstract

Bu çalışmada önce, farklı primer ve sekonder aminlerin ditiyokarbamat tuzları, 1,3-dikloraseton ile etkileştirildi. Daha sonra tiyazol-2-tiyon ve alkilditiyokarbamat esterleri sentezlendi. Yeni bileşiklerin kimyasal yapıları FT-IR, 1H-NMR, 13C-NMR spestroskopik metotları ve elementel analiz tekniği ile belirlendi.

Keywords

Ditiyokarbamat tuzları α-Haloketon Tiyazol-2-tiyon.

References

  • Buschand, M., Starke, M., J. Prakt. Chem., 93, 49, 1916.
  • Metzger, J. V., John Wiley and Sons, 34, 1979.
  • Desai, N. C., Indian J. of Chem., 32B, 343-346, 1993.
  • Melendez, E., Merchen, F. L., Merino, P., J. Het. Chem., 28, 653, 1991.
  • Katritzkyand, A. R., Bayyuk, S., Heterocycles, 23, 12, 1985.
  • Katritzky, A. R., Tarr, R. D., J. of Poly. Sci. Part A: Pol. Chem., 25, 3205, 1987.
  • Miolati, A., Gazz. Chem. İtal., 23, 575, 1893.
  • Amico, J. J. D., Bollingerand, F. G., Freeman, J. J., J. Het. Chem., 23, 101, 1986.
  • Molina, P., Arques, A., Velascoand, M. de los D., Villialgordo, J. M., Heterocycles, 26, 5, 1987.
  • Katritzky, A. R., BorowieckaandWei-Qieng Fan, J., J. Het. Chem., 28, 1139, 1991.
  • Erten, M., Tayhan, A. B., Yulug, N., Arch. Pharm., 323, 605-609, 1990.

The Reaction of Alkyldithiocarbamate Salts with 1,3-Dichloroacetone

Year 2016, Volume: 6 Issue: 1, 44 - 51, 30.06.2016

Cumhur Kırılmış Esra Barım

Abstract

In this study, dithiocarbamatesalts of different primary and secondary amines were firstly interacted with 1,3-dichloroacetone. Then, thiazole-2-thione and alkyldithiocarbamate esthers were synthesized. The chemical structures of the new compounds were determined by FT-IR, 1H-NMR, 13C-NMR spectroscopic methods and elemental analysis technique.

Keywords

Dithiocarbamatesalts α-Haloketone Thiazole-2-thione.

References

  • Buschand, M., Starke, M., J. Prakt. Chem., 93, 49, 1916.
  • Metzger, J. V., John Wiley and Sons, 34, 1979.
  • Desai, N. C., Indian J. of Chem., 32B, 343-346, 1993.
  • Melendez, E., Merchen, F. L., Merino, P., J. Het. Chem., 28, 653, 1991.
  • Katritzkyand, A. R., Bayyuk, S., Heterocycles, 23, 12, 1985.
  • Katritzky, A. R., Tarr, R. D., J. of Poly. Sci. Part A: Pol. Chem., 25, 3205, 1987.
  • Miolati, A., Gazz. Chem. İtal., 23, 575, 1893.
  • Amico, J. J. D., Bollingerand, F. G., Freeman, J. J., J. Het. Chem., 23, 101, 1986.
  • Molina, P., Arques, A., Velascoand, M. de los D., Villialgordo, J. M., Heterocycles, 26, 5, 1987.
  • Katritzky, A. R., BorowieckaandWei-Qieng Fan, J., J. Het. Chem., 28, 1139, 1991.
  • Erten, M., Tayhan, A. B., Yulug, N., Arch. Pharm., 323, 605-609, 1990.
There are 11 citations in total.

Details

Journal Section Chemistry
Authors

Cumhur Kırılmış

Esra Barım

Publication Date June 30, 2016
Submission Date February 8, 2016
Published in Issue Year 2016 Volume: 6 Issue: 1

Cite

APA Kırılmış, C., & Barım, E. (2016). The Reaction of Alkyldithiocarbamate Salts with 1,3-Dichloroacetone. Adıyaman University Journal of Science, 6(1), 44-51.
AMA Kırılmış C, Barım E. The Reaction of Alkyldithiocarbamate Salts with 1,3-Dichloroacetone. ADYU J SCI. June 2016;6(1):44-51.
Chicago Kırılmış, Cumhur, and Esra Barım. “The Reaction of Alkyldithiocarbamate Salts With 1,3-Dichloroacetone”. Adıyaman University Journal of Science 6, no. 1 (June 2016): 44-51.
EndNote Kırılmış C, Barım E (June 1, 2016) The Reaction of Alkyldithiocarbamate Salts with 1,3-Dichloroacetone. Adıyaman University Journal of Science 6 1 44–51.
IEEE C. Kırılmış and E. Barım, “The Reaction of Alkyldithiocarbamate Salts with 1,3-Dichloroacetone”, ADYU J SCI, vol. 6, no. 1, pp. 44–51, 2016.
ISNAD Kırılmış, Cumhur - Barım, Esra. “The Reaction of Alkyldithiocarbamate Salts With 1,3-Dichloroacetone”. Adıyaman University Journal of Science 6/1 (June 2016), 44-51.
JAMA Kırılmış C, Barım E. The Reaction of Alkyldithiocarbamate Salts with 1,3-Dichloroacetone. ADYU J SCI. 2016;6:44–51.
MLA Kırılmış, Cumhur and Esra Barım. “The Reaction of Alkyldithiocarbamate Salts With 1,3-Dichloroacetone”. Adıyaman University Journal of Science, vol. 6, no. 1, 2016, pp. 44-51.
Vancouver Kırılmış C, Barım E. The Reaction of Alkyldithiocarbamate Salts with 1,3-Dichloroacetone. ADYU J SCI. 2016;6(1):44-51.

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